Compressive performance of MAX phase composites

Compressive performance and crack propagation in MAX phase composites 

Here micro CT was used to reveal the structure performance relationships in metal/ceramic composites based on Ti2AlC / Al alloy combinations.

The results show the promise of infiltrated max phase materials in the production of high performance composites.

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Abstract

Composite materials comprising a porous Ti2AlC matrix and Al 6061 alloy were fabricated by a current-activated pressure assisted melt infiltration process. Coarse, medium and fine meso-structures were prepared with Al alloy filled pores of differing sizes. Materials were subjected to uniaxial compressive loading up to stresses of 668 MPa, leading to the failure of specimens through crack propagation in both phases. As-fabricated and post-failure specimens were analysed by X-ray microscopy and electron microscopy. Quasi-static mechanical testing results revealed that compressive strength was the highest in the fine structured composite materials. While the coarse structured specimens exhibited a compressive strength of 80% relative to this. Reconstructed micro-scale X-ray tomography data revealed different crack propagation mechanisms. Large planar shear cracks propagated throughout the fine structured materials while the coarser specimens exhibited networks of branching cracks propagating preferentially along Al alloy-Ti2AlC phase interfaces and through shrinkage pores in the Al alloy phase. Results suggest that control of porosity, compensation for Al alloy shrinkage and enhancement of the Al alloy-Ti2AlC phase interfaces are key considerations in the design of high performance metal/Ti2AlC phase composites.